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Joined: 19 Mar 2008. Location: United States Online Status: Offline Posts: 36, Quote snufse Reply bullet Topic: QR Codes Posted: 02 May 2012 ...
(or bases) that are equivalent in water.] Thus, they can be determined separately by titration. Moreover, in such a solvent, some bases, which are too weak to titrate in water, can be titrated and their strengths can be determined. (ii) In solvents with a wide pH region on the right, the lyate ion (S ) has very strong basicity and some bases, which behave as strong bases in water, tend to behave as weak bases of different strengths. They can be determined separately by titration. Moreover, in such a solvent, some acids, which are too weak to titrate in water, can be titrated and their strengths can be determined. In protophobic aprotic solvents, the pH window expands on both sides and all of the advantages in (i) and (ii) can be realized. Figure 3.7 shows the titration curve for a mixture of several acids in 4-methyl-2-pentanone (MIBK). In the figure, HClO4 and HCl, which are strong acids in water, are differentiated, and phenol, which is a very weak acid, can accurately be determined [21]. Acid-base titrations in non-aqueous solvents have wide applicabilities [1, 3, 22]. The titrations are especially useful in determining medicinal substances, because many of them are weak acids or bases. The indicator method can be used to detect end-points. However, potentiometric titrations that use a pH meter, a pH sensor and an automatic burette are most useful. Valuable physicochemical information, including acid dissociation constants, can be obtained from potentiometric titration curves ( 6). The hydrogen ion in protophobic aprotic solvents is very reactive. For example, judging from the values of transfer activity coefficient, H+ in AN is 108 times more reactive than in water. Thus, if basic substances are added to the solution in AN, they easily combine with H+. Table 3.6 shows the complex formation con- qr code crystal reports 2008 QR Code Generator in Crystal Reports - KeepAutomation.com
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